DOI: 10.1039/d6fd00089d ISSN: 1359-6640
Optimisation of measurement and data analysis of time-resolved X-ray absorption spectroscopy of thin film organic semiconductors
Belen Alonso-Garcia, Miguel M. Manresa-Nalda, Oliver G. Alexander, Kaiyu Hu, Felix S. Egun, Zachery Donnellan, Joseph J. Broughton, Jacob P. Lee, David J. Hoffman, Kristjan Kunnus, Matt Bain, Douglas Garratt, Oliver Gessner, Mary R. Matthews, Jon P. MarangosCombining dose-aware experimental design with shot-resolved regression enables reliable fluorescence-detected XAS in soft X-ray XFEL experiments on dose-limited samples, reducing run-to-run spectral variability by up to 4.4-fold.