DOI: 10.1039/d6ob01129b ISSN: 1477-0520

Continuous flow electrochemical oxidation of activated methylarenes using O 2

Noura Alqahtani, Suguru Iwai, Tribani Boruah, Rebecca L. Melen, Thomas Wirth

Selective benzylic C–H oxidation to aldehydes is achieved in flow using O 2 , where efficient gas–liquid mass transfer suppresses overoxidation and oxidation potentials dictate reactivity, enabling a sustainable, catalyst-free process.

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