DOI: 10.1002/adfm.202310140 ISSN: 1616-301X

A Highly Soluble Iron‐Based Posolyte Species with High Redox Potential for Aqueous Redox Flow Batteries

Jinxu Gao, Kyumin Lee, Kiana Amini, Roy G. Gordon, Theodore A. Betley, Michael J. Aziz
  • Electrochemistry
  • Condensed Matter Physics
  • Biomaterials
  • Electronic, Optical and Magnetic Materials

Abstract

A novel iron‐based posolyte redox species are presented for an aqueous redox flow battery, (Tetrakis(2‐pyridylmethyl)ethylenediamine)iron(II) dichloride, which is obtained by a simple synthetic route, shows a high redox potential of 0.788 V versus SHE, and exhibits exceptional aqueous solubility of 1.46 M. Paired with bis(3‐trimethylammonio)propyl viologen tetrachloride at neutral pH, the battery demonstrates an open‐circuit voltage of 1.19 V and delivers good cycling performance, with a capacity fade rate of 0.28% per day and coulombic efficiency of 99.3%. Postmortem chemical and electrochemical analyses of the posolyte species suggest future routes for stabilization of the complex. Among all the iron complexes with a redox potential above 0.4 V versus SHE, this compound exhibits the highest solubility. These results offer valuable insights that can be applied to the development of future posolyte species for sustainable energy storage solutions.

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